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live

I love to listen live music - some songs sound much brighter, richer and deeper than it was in live performance, studio recording is sometimes err stereotyped excessive accuracy, the lack of spontaneous improvisation. Therefore, if possible try to get out to the concerts of my favorite bands and artists! Decided to recall all those I have seen and heard in Live from 2004!
Deep Purple, Uriah Heep, Queen + Paul Rogers, Paul McCartney - still left a good impression after a concert musicians, formed the my taste. Of special note is also speech Beyonce - amazing quality, skill of execution!
Among the Ukrainian group, demonstrated Okean Elzy, BB, Esthetic Education, Fleur, Boombox. Из русских пока лишь Алиса была увидена и услышана, ну а Brainstorm представили мне прибалтийскую сцену!
В планах: Muse, the Killers, Jon Lord. Это как минимум.

А кого вы слушали в живую?

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ozdvignut monument in 1932 near the gate of Pius.

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Locman

More recently came out of nowhere I have a cult of wristwatches. Beautiful chronographs from Timex and Tissot, rabid Hurricanes Swiss Military, huge sverhfunktsionalnye Pathfinder and bulletproof G-Shock from Casio took my brain! Recently stumbled upon known (as it turned out!) brand of Italian hours Locman , have signed a contract with the Italian army, and issued on the Mount series of wonderful hours Militari: for naval Forces Italy (Marina Militare), Air Force (Aeronautica), for my favorite Parachute Brigade Folgore, as well as "admiral" (Ammiraglio).
particularly good first


and laconic pilot for Italian BOPLov, named after the legendary submariner during World Theseus Tezei

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King Crimson

Their music is still a mystery to me. I do not get tired wonder Fripp and his tvrchestvu, and can hardly imagine what the mechanism of functioning of his mental processes that give rise to such a strange unusual music. Guitarist crimson king created his own world, whose faces are gradually opening up while listening to his magical compositions.

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Boredom and merlot

Here we are, three degrees below zero, resisting the urge to kick me in bed doing nothing. On the bedside table waiting for me a book that I did not want to read. The evening are Internet users already finished at eleven and a quarter, and almost back again to attack the boredom. The feel that I bring them around without hovering, as if he was playing with me. It 'hard, go on.

But the important things. Because I have little desire to write.

Nell'intossicazione from drunkenness I found the courage to confront face to face what I'm escaping for a long time. Too, of course. And somewhere, even if you do not know where, I must find the strength to fight back and start again. Not torture, but even look at him.

But I lie, I lie straight to the mirror / The one I've broken to match my face

Mh.

So, the important things.

I'm afraid.

I worked so much last year, only to bury their heads in piles of things to do. I killed her for not thinking, and cabbage if it worked!
Not now, not so. Now breath too, I too airy spaces and vast that I can not lock into any box. And my palms are empty, and everything is too monotonous. Now I fear gripped
2013. Which has the form of abandonment, of a term for something that after all I is willing to go into the unknown, the victory or failure, the real comparison - finally - with the life I've been waiting for.

I feel surprisingly tired, old but not defeatist. I still have your whole life ahead, but I do not feel better on the skin. What has happened? It 'was this serene easy to circumvent? I do not know what to think of quell'elettrizzante carefree, except that now the game is difficult, and I do not have the forces to dominate. So I have to close your eyes, take a breath, focus and take things as I always did when they were too enormous to be addressed: one step at a time. I may start from here.

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how chuvstvoval!:)

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knockwave @ 2010-12-16T19: 13:00

Dear Santa... Dear Santa, This year I've been busy! Last Friday I donated bone marrow to ladyaethelflaed in a life-saving procedure (300 points) . In August I set livin_derevel 's puppy on fire (-66 points) . Last Thursday I gave tommykaine a kidney (1000 points) . In March I bought porn for baka_chibitalia (-10 points) . In October I gave baka_chibitalia a life-saving blood transfusion (50 points) . Overall, I've been nice (1274 points) . For Christmas I deserve an Easy-Bake Oven ! Sincerely, knockwave

Write your letter to Santa! Enter your LJ username:

hahahah XD
preso da tommykaine   XD

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salt made in home

come promesso, oggi is Sunday and posed a cool thing XD
chemistry in this post I will explain how to make rooms in the house!
have this caustic soda? the ultra-corrosive substance that corrodes you if you touch it? here is the first ingredient!
the second ingredient is hydrochloric acid, commercially known as muriatic acid, also ultra corrosive!
now, the recipe:
Dissolve soda in water (measured accurately the weight of soda before you put it in water), then add about 90 ml of hydrochloric acid for every 10 grams of soda dissolved in water.
at this point put the container in a place where you can evaporate all the water and when there will not be more on the bottom of your container with a layer of pure salt!
now I explain why two dangerous substances give a completely harmless substance if mixed:
the chemical formula of soda is NaOH, the acid is HCl and the salt is NaCl.
hours, the chemical reaction is: NaOH + HCl -> NaCl + H2O
NaCl is the salt, H2O is water, so that eventually evaporates.
sincerely do not recommend it because it costs more to buy the salt at the supermarket
XD but if you want to do all you need to use the task of weighing the soda and the addition of the protective gloves (latex, rubber, whatever you want) and if you paid in error on something immediately wash under running water.
I recommend it if you do be very careful and do it in the sink!
ok, next week with the next cool thing! ^ ^

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first experience in the laboratory

today I finished the first lab experience, then share it with you!

experience consisted in the separation of benzoic acid and α-tetralone from a mixture.
first are taken slowly with a 50 ml graduated cylinder (figure).

the mixture is transferred into a separating funnel 250 ml, attached to the racks under the hood with a ring (figure).

at this point are taken with a graduated cylinder 50 ml of ethyl acetate (a solvent) which is poured into the funnel to dilute the solution.
hours are taken 100 ml of water and pour them into a beaker, where it is dissolved 5 g of NaOH, better known as caustic soda.
this basic solution is used to initiate the separation: in fact, in two shifts with 50 ml of solution is poured into the separating funnel, the shakes and it vents to let out the gas formed, then puts the funnel in 'ring, and it expects to separate two phases in the aqueous solution will be dissolved with sodium benzoate (salt that is formed by reaction of benzoic acid and sodium carbonate), there will be over the ethyl acetate with α-tetralone.
removing the aqueous phase through the tap funnel, letting it drip into a 250 ml beaker until there is more than the funnel, while the organic phase is left behind protected by a cap to prevent contamination .
prepares a bath in ice in a recrystallized (figure) gets crushed ice and add a bit 'of water.

there we enter the beaker with sodium benzoate, then get ready to party 20 ml of 6 N (normal) HCl (hydrochloric acid): starting from a standard solution 12 N, if they take 10 ml, which are then elongated with 10 ml of water.
the acidic solution is added very slowly to the solution through a Pasteur pipette with benzoate (figure), until it reaches an acidic pH (below 2) and is controlled with the aid of a litmus test.

at this point benzoic acid reformed is not very soluble in water, so it falls into a whitish powder, which must be filtered.
filtration prepare a filter paper for Buchner, which is placed on a flask Tailed attached to the water pump vacuum (figure). water pump is nothing more than a double outlet pipe connected to the sink: when you open water, its movement causes a "suction" in the other exit of the tube, sucking air and creating a vacuum.

to filter the sour, pour the solution into the Buchner and washed the residue with a little 'cold water (taken from the ice bath), then moved the solid acid in a 250-ml flask and add 40 \\ 50 ml of water to dissolve it again.
you put a glass rod into the flask and mounting the condenser (figure), which is connected to the tap to let water in and get it out from above.

you put the ball in termomanto (figure), which goes on, stirring occasionally to dissolve completely benzoic acid, for then allow it to recrystallize. This method, called recrystallization, is used to remove the last traces of impurities by acid benzoic acid.
(sorry, I could not find a better ... the blue car with termomante is inside the ball) when the acid recrystallized
, died on termomante and moved the ball in an ice bath to complete recrystallization.
is filtered again and moved on Buchner acid obtained in a previously weighed recrystallized, then putting it in the oven overnight to remove all traces of water.
when he is out of the stove, it is weighed to see how much acid has been recovered, then we move on to testing for purity: melting point, TLC (thin layer chromatography) analysis and IR (infrared).
to the melting point gets a little sample in a special capillary sealed at the bottom and it also puts them in a special machine that heats slowly until the stops, recording the melting temperature shown on the display.
preparing the plates for TLC by drawing a line about 1 \\ 1.5 cm from the bottom and drawing three dots to the order, the sample, reference and pure mixture of departure, which should be placed in 3 tubes (the sample and the reference, being solid, be dissolved with a little 'methylene chloride).
you cut a piece of paper the size of the jar that you will use (you need to see better) and pour into 10 ml of a solution costutita 8 ml of petroleum ether and 2 ml of ethyl acetate (this solution is called eluent).
lay it down on the plate with a capillary sample, the reference and the mixture, then put into the jar and let the eluent, by capillary action, the soak, pulling out only when the eluent has come to 1 \\ 2 cm from the top, marking the exact spot with a pencil (used for the calculation of RF, retention factor: distance from the point of deposition of stain / total distance of the eluent).
few seconds after the slide is again dry because the eluent evaporates quickly, so I can put it under a UV lamp and mark the spots (figure).
(left to right: sample and reference mixture. Benzoic acid stain is stretched down, while the stain on the Misel is the α-tetralone)
finally prepares the sample for ' IR analysis: a small part of the sample is placed in an agate mortaietto with a little paraffin oil (the sample must be the majority) and the pesto until it reduces to a uniform pap, from which a sample is taken to be laid on a special slide NaCl (table salt), which closes with the other half. I put this all in the sample holder and the machine for the IR analysis connected to the computer that you want to print a chart (figure).

now back to the organic phase: you should wash with a saturated solution of NaCl, which is prepared by adding salt to the water until it is a bit 'on the bottom.
separating funnel to pour twice 50 ml of NaCl, shakes and outgassing, then removing the aqueous phase (below).
recovered organic phase is freed of a lot of residual water in a flask, where it adds to anidrificare sodium sulphate, stirring and adding until it is dusty, a sign that has absorbed all water.
you filter with a pleated filter in a funnel (figure), taking the organic phase dried in a balloon.

rotavapor attaches to the ball (figure) and I switch it on, all the solvent to evaporate.

weigh an empty flask and attaching it to a Vigreux distillation flask as recovery, attacking each other at the beginning so that its contents are distilled, you insert the thermometer with a Quickfit (stopper particular) and a capillary break the boil. I position the ball with the solution in termomanto and attack all at a vacuum gauge and a vacuum pump; connection pipes for water and open the tube (figure).
(sorry, I have not found anything better ...)
recovery I put the ball in an ice bath to help condense the distillate.
when the first drop there is marked falls in temperature and pressure boiling.
at the end of the distillation, the flask with weight recovery dell'α-pure tetralone.
Now make a plate for the TLC and we put it on the sample, the reference (diluted in methylene chloride) and the mixture of departure (figure).
(as before I left: standard, reference and mixture)
Finally, I put a drop of pure sample on the slide to make the IR analysis, taking the press (figure).


and with this I concluded, if you have any questions just ask!

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^ ^ ok, I know I'm late, but I did it on purpose, I've been busy XD
in any event, as promised, now talk about the dry ice *-*

then, to start from a Photo:

this is the typical appearance of dry ice. ice seems normal, if it were not for the form (the cylinders are very small) and the fact that gas emanates.
dry ice is called in this way just because it seems the ice, but it is not at all: it does not contain a single drop of water.
is nothing but solid carbon dioxide. exact, that very gas that is emitted as a waste of breath, which is produced by burning organic compounds and promotes the greenhouse effect.
how do you turn a gas into a solid? it cools to the freezing point. atmospheric pressure the carbon dioxide passes directly from gas phase to solid phase without an intermission liquid at a temperature of -78 ° C. please, do not ever touch it with bare hands or you ustionerà!
at room temperature tends to go back to the gas from the solid phase and that is why we always see a little bit of smoke around it.
if we blow above, as the breath of the air is warmer, more gas is released, producing a kind of white mist, ditto when you put it in water.
theater, cinema or in the shows is typically used to make the fog: in fact, if you throw in ethanol (known as "alcohol pink disinfectant, which is essentially the same alcohol you drink beverages just alcohol) creates a dense white mist:

cool, right? *-*
wanting it can be bought in a shop that sells chemicals or the like, it costs a little bit, but the effect Dense fog is guaranteed!
fact carbon dioxide is denser and heavier air, and thus tends to move downwards, as shown in the photo, causing an effect much like especially to producers of horror films is not easy XD
be retained, however, because at any temperature above -78 ° C tends to return to gas, thus serving containers insulation (like the thermos, but even more insulating) or special freezer (the temperature rarely reaches the house to infieriori -10 ° C).
in chemistry is used to maintain very low temperatures because it is quite solid (if not force it takes a little 'time to sublimate all), same for physics. in physics, moreover, is also used in experiments in which we must "undo" the friction, because a layer of gas between the plane and the body you want to move without friction.
is also used in the food for storage and transport of food.
in the medical field is used, they tended to maintain low temperature.
can also be used to clean and smooth surfaces: if a shot at high speed against a surface, in fact, yields The same as common sand, but without residual gas to come quickly and more accurately than the blast itself. for example, is used to clean the mirrors of the telescope of the Astrophysical Observatory on Mauna Kea in Hawaii, where even the smallest defect of mirrors can make the wrong data.
in an experiment done at a fair orientation with my fellow students we have found that putting it in the water makes it slightly fizzy XD
dry ice is completely non-toxic, unless it is excessive concentration in a room closed and not ventilated, then it may stifle because it replaces the oxygen in the blood, but otherwise causes no problems of any kind.
ok, I would say that I have talked enough dry ice, if you have any questions just ask in the comments!
next week with another cool thing in chemistry! ^___^

Levelling Collimation

working.

Fatigue terrible that I take these days, sinking. I have little energy - and invaluable - to do very little, but very intensely. I'm trying to do my best, and that's what counts. Always.

Always.

This is what I was taught, at least. What I feel inside me today is something different, maybe.
The desire to emerge. The desire to be able to pursue a desire. The feeling of not being quite high flying, fear of Starla doing.
So many things are mixed, leaving him this feeling heavy. As chains from which escape. Weights leave the ground to soar into the sky, up there.

Great work. Great effort. Projects that are still all in the mind, and that could ... Who knows? could perhaps be realized, if I can stay in here, in the now. A commitment now, because even if the mind is ahead, the work here is not even halfway.

All this desire for novelty must bend, now under the hard work. Once the workout is all downhill.

And down.

-

I'm just so tired. And that's why I Simply can not translate what I wrote here ... It's not that I do not want, it's that's just stupid. One can not translate word by word His thoughts. From a language to the other, like D. did with his website. One can just try to rewrite them under another form. In another, different way.

So, I'm tired. But I'm doing good stuff, so I'm satisfied, too. In the past few days I've realized that I need to work out for what I wish to do. "Dream" is a huge word for what I like to call a mere 'project'. Without any capital letter, yeah. Just a project, nothing else.
A project that make my eyes sparkle.
A project that I'd really like to realize.
A project that's just a project. Yeah. Nothing else, really.

Her words made me think about it. And I realized that I still need to learn A lot of things, before Being ready to go ahead. It Could Be Already late, but I'm ready to fight to see my project Realized, and I think I Still Have A Few aces up my sleeves. I will not underrate the toughness of this way again, like I used to do.

And that's the very first step Towards victory.

New

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dry ice lab laboratory

ok, not kill me, but the experience the finish Thursday ò ì 9 because it is too long and today we are not managed to finish , then 'll post the report next Thursday XD
however Sunday put or a nice post dedicated a. ..* roll of drums *... Dry ice ! *-*

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nothing, today jumped all because of snow ... If I had known I would not even come in one since I skipped the lessons because we are too few è_é